Reduction of phosphine oxides to phosphines with the InBr3/TMDS system
Identifieur interne : 001619 ( Main/Repository ); précédent : 001618; suivant : 001620Reduction of phosphine oxides to phosphines with the InBr3/TMDS system
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Abstract
An efficient method for the reduction of phosphine oxide derivatives into their corresponding phosphines is described. The system InBr3/TMDS allows the reduction of different secondary and tertiary phosphine oxides as well as aliphatic and aromatic phosphine oxides.
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<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en" level="a">Reduction of phosphine oxides to phosphines with the InBr<sub>3</sub>/TMDS system</title><author><name sortKey="Pehlivan, Leyla" uniqKey="Pehlivan L">Leyla Pehlivan</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>Laboratoire de Catalyse et Synthese Organique, Institut de Chimie et Biochimie Moleculaires et Supramoleculaires (ICBMS), CNRS, UMR5246, Université Lyon 1, 43 Boulevard du 11 Novembre 1918, Bat CPE</s1><s2>69622 Villeurbanne</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>5 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Rhône-Alpes</region><settlement type="city">Villeurbanne</settlement></placeName></affiliation></author><author><name sortKey="Metay, Estelle" uniqKey="Metay E">Estelle Metay</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>Laboratoire de Catalyse et Synthese Organique, Institut de Chimie et Biochimie Moleculaires et Supramoleculaires (ICBMS), CNRS, UMR5246, Université Lyon 1, 43 Boulevard du 11 Novembre 1918, Bat CPE</s1><s2>69622 Villeurbanne</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>5 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Rhône-Alpes</region><settlement type="city">Villeurbanne</settlement></placeName></affiliation></author><author><name sortKey="Delbrayelle, Dominique" uniqKey="Delbrayelle D">Dominique Delbrayelle</name><affiliation wicri:level="3"><inist:fA14 i1="02"><s1>Minakem SAS, 145 Chemin des Lilas</s1><s2>59310 Beuvry la Foret</s2><s3>FRA</s3><sZ>3 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Nord-Pas-de-Calais</region><settlement type="city">Beuvry la Foret</settlement></placeName></affiliation></author><author><name sortKey="Mignani, Gerard" uniqKey="Mignani G">Gerard Mignani</name><affiliation wicri:level="3"><inist:fA14 i1="03"><s1>Rhodia, Lyon Research center, 85, Avenue des Freres Perret, BP 62</s1><s2>69192 Saint-Fons</s2><s3>FRA</s3><sZ>4 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Rhône-Alpes</region><settlement type="city">Saint-Fons</settlement></placeName></affiliation></author><author><name sortKey="Lemaire, Marc" uniqKey="Lemaire M">Marc Lemaire</name><affiliation wicri:level="3"><inist:fA14 i1="01"><s1>Laboratoire de Catalyse et Synthese Organique, Institut de Chimie et Biochimie Moleculaires et Supramoleculaires (ICBMS), CNRS, UMR5246, Université Lyon 1, 43 Boulevard du 11 Novembre 1918, Bat CPE</s1><s2>69622 Villeurbanne</s2><s3>FRA</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>5 aut.</sZ></inist:fA14><country>France</country><placeName><region type="region" nuts="2">Rhône-Alpes</region><settlement type="city">Villeurbanne</settlement></placeName></affiliation></author></titleStmt><publicationStmt><idno type="inist">12-0259155</idno><date when="2012">2012</date><idno type="stanalyst">PASCAL 12-0259155 INIST</idno><idno type="RBID">Pascal:12-0259155</idno><idno type="wicri:Area/Main/Corpus">001C32</idno><idno type="wicri:Area/Main/Repository">001619</idno></publicationStmt><seriesStmt><idno type="ISSN">0040-4020</idno><title level="j" type="abbreviated">Tetrahedron : (Oxf. Print)</title><title level="j" type="main">Tetrahedron : (Oxford. Print)</title></seriesStmt></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Aliphatic compound</term><term>Aromatic compound</term><term>Chemical reduction</term><term>Indium bromide</term><term>Organic phosphine</term><term>Phosphorus Organic compounds</term><term>Tertiary phosphine oxide</term></keywords><keywords scheme="Pascal" xml:lang="fr"><term>Réduction chimique</term><term>Phosphine organique</term><term>Bromure d'indium</term><term>Phosphine tertiaire oxyde</term><term>Composé aliphatique</term><term>Composé aromatique</term><term>Phosphore Composé organique</term><term>Phosphine oxyde</term><term>Disiloxane(tétraméthyl)</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">An efficient method for the reduction of phosphine oxide derivatives into their corresponding phosphines is described. The system InBr<sub>3</sub>/TMDS allows the reduction of different secondary and tertiary phosphine oxides as well as aliphatic and aromatic phosphine oxides.</div></front></TEI><inist><standard h6="B"><pA><fA01 i1="01" i2="1"><s0>0040-4020</s0></fA01><fA02 i1="01"><s0>TETRAB</s0></fA02><fA03 i2="1"><s0>Tetrahedron : (Oxf. 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All rights reserved.</s1></fA44><fA45><s0>23 ref.</s0></fA45><fA47 i1="01" i2="1"><s0>12-0259155</s0></fA47><fA60><s1>P</s1></fA60><fA61><s0>A</s0></fA61><fA64 i1="01" i2="1"><s0>Tetrahedron : (Oxford. Print)</s0></fA64><fA66 i1="01"><s0>GBR</s0></fA66><fC01 i1="01" l="ENG"><s0>An efficient method for the reduction of phosphine oxide derivatives into their corresponding phosphines is described. 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